A Heterogeneous, Highly Efficient, and Reusable Mo-Al2O3 Composites Based Organocatalyst for One Pot Three-Component Mannich Reaction for the Synthesis of β-aminocarbonyl Compounds
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Published:2023-01-02
Issue:
Volume:
Page:234-241
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ISSN:1984-6428
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Container-title:Orbital: The Electronic Journal of Chemistry
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language:
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Short-container-title:Orbital: Electron. J. Chem.
Author:
Thirunarayanan GanesamoorthyORCID,
Anam Koteswara Rao
Abstract
We have successfully developed a new Mo-Al2O3/p-TSA organocatalyst which has improved the yield of the Mannich reaction. This protocol has the advantage of mild conditions, high yield, easy work-up, environmentally friendly procedure, and the solid catalyst was recycled. The catalyst was analysed by XRD, SEM, and EDS techniques. The synthesized Mo-Al2O3composites were used in the presence of p-toluene sulfonic acid (p-TSA) conducts the one-pot three-component Mannich reaction and various β-amino ketones prepared with good yields and characterized by IR, 1H, and 13C NMR Techniques.
Publisher
Instituto de Quimica - Univ. Federal do Mato Grosso do Sul
Subject
Materials Science (miscellaneous),General Chemical Engineering,General Chemistry