Experimental study on the rheological characteristics and viscosity-enhanced factors of super-viscous heavy oil

Abstract

To reveal the viscosity-enhanced mechanism of super-viscous heavy oil and improve the recovery rate of super-viscous heavy oil, the four components, elemental composition, rheological properties, and effects of asphaltenes and resin on the viscosity of super-viscous heavy oil from well TH12434 in Tahe Oilfield, China have been analyzed from macro and microscopic perspectives by Anton Paar rotational rheometer, gas chromatography-mass spectrometry and scanning cryo-EM to solve the problems of poor fluidity and high asphaltene content. The experimental results showed that in the temperature range of T= 40-100°C, the viscosity of super-viscous heavy oil decreases sharply from 352000 mPa∙s to 1620 mPa∙s, and the super-viscous heavy oil exhibits clear thermo-sensitivity. With T= 100°C and shear rate ranging from γ= 0-800 s-1, the viscosity of super-viscous heavy oil decreases sharply from 45000 mPa∙s to 956 mPa∙s, and the oil sample shows typical pseudoplasticity. The baseline of super-viscous heavy oil analysis by gas chromatography shows too high, and more than 80 % of super-viscous heavy oil compounds have a matching degree of less than 70 % with standard compounds, indicating that the super-viscous heavy oil had poor heterogeneity and many impurities. It is observed by scanning cryo-EM that the micromorphology of super-viscous heavy oil is large granular, strong continuity, asphaltene micromorphology presents an obvious layered structure, the layer spacing is 637.7 nm, and its asphaltene molecules form an order-like or crystal-like association structure through several unit sheet layers, resulting in high viscosity of super-viscous heavy oil. Based on the analysis results of the influencing factors of the viscosity of super-viscous heavy oil, a theoretical basis for the selection of viscosity reduction technology for super-viscous heavy oil the efficient exploitation in Tahe Oilfield, China could be provided.