Accurate extrinsic and intrinsic peak broadening modelling for time-resolved <i>in situ</i> ball milling reactions <i>via</i> synchrotron powder X-ray diffraction-Reference-Cited by-同舟云学术

Accurate extrinsic and intrinsic peak broadening modelling for time-resolved in situ ball milling reactions via synchrotron powder X-ray diffraction

Published:2023 Issue: Volume:241 Page:289-305
ISSN:1359-6640
Container-title:Faraday Discussions
language:en
Short-container-title:Faraday Discuss.

Author:

Mazzeo Paolo P.¹²^ORCID,Lampronti Giulio I.³^ORCID,Michalchuk Adam A. L.⁴^ORCID,Belenguer Ana M.⁵^ORCID,Bacchi Alessia¹²^ORCID,Emmerling Franziska⁴^ORCID

Affiliation:

1. Department of Chemistry, Life Sciences and Environmental Sustainability, University of Parma, Parco Area Delle Scienze 17/A, Parma 43124, Italy

2. Biopharmanet-TEC, University of Parma, Parco Area Delle Scienze 27/A, Parma 43124, Italy

3. Department of Materials Science & Metallurgy, University of Cambridge, 27 Charles Babbage Rd, Cambridge CB3 0FS, UK

4. BAM Federal Institute for Materials Research and Testing, Richard-Willstätter-Straße 11, D-12489 Berlin, Germany

5. Yusuf Hamied Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, UK

Abstract

A state-of-the-art Rietveld refinement strategy is proposed to derive the instrumental resolution function (IRF) for a ball-mill setup for time-resolved in situ (TRIS) synchrotron XRPD.

Funder

Ministry of Education, Universities and Research

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2023/FD/D2FD00104G

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