Metal-free C(sp3)–H functionalization (C–C and C–N bond formation) of 1,2,3,4-tetrahydroacridines using deep eutectic solvents as catalyst and reaction medium

Author:

Shirisha Thangellapally1,Majhi Subir1,Balasubramanian Sridhar23,Kashinath Dhurke1ORCID

Affiliation:

1. Department of Chemistry, National Institute of Technology, Warangal-506 004, India

2. Centre for X-ray Crystallography, Department of Analytical & Structural Chemistry, CSIR-Indian Institute of Chemical Technology, Tarnaka, Uppal Road, Hyderabad-500007, Telangana, India

3. Academy of Scientific and Innovative Research (AcSIR), Ghaziabad-201 002, India

Abstract

A simple and efficient protocol for the addition of azodicarboxylates (C–N bond) and maleimides (C–C bond) at the C4-position of 1,2,3,4-tetrahydroacridines was achieved under metal-free conditions using deep eutectic solvents with high atom efficiency, regioselectivity, and yields.

Funder

Ministry of Education, Government of India

Science and Engineering Research Board

Publisher

Royal Society of Chemistry (RSC)

Subject

Organic Chemistry,Physical and Theoretical Chemistry,Biochemistry

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