Improved on-line benchtop 31P NMR reaction monitoring via Multi-Resonance SHARPER-Reference-Cited by-同舟云学术

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Improved on-line benchtop ³¹P NMR reaction monitoring via Multi-Resonance SHARPER

Published:2024 Issue:31 Volume:16 Page:5399-5402
ISSN:1759-9660
Container-title:Analytical Methods
language:en
Short-container-title:Anal. Methods

Author:

Tadiello Laura¹²,Halse Meghan E.²^ORCID,Beweries Torsten¹^ORCID

Affiliation:

1. Leibniz Institute for Catalysis (LIKAT), Albert-Einstein-Str. 29a, 18059 Rostock, Germany

2. Department of Chemistry, University of York, YO10 5DD, York, UK

Abstract

On-line reaction monitoring of hydrogenation reactions of oxygen-sensitive organometallic complexes is done via a 31P benchtop NMR spectrometer using the Multi-Resonance Sensitive Homogeneous And Resolved PEaks in Real time (MR-SHARPER) sequence.

Funder

Engineering and Physical Sciences Research Council

Deutsche Forschungsgemeinschaft

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/AY/D4AY00948G

Reference18 articles.

1. J. F.Hartwig , Organotransition Metal Chemistry. From Bonding to Catalysis , University Science Books , Sausalito , 2010 ; A. L.Clevenger , R. M.Stolley , J.Aderibigbe , J.Louie , Chem. Rev. 2020 , 120 , 6124–6196 ; S.Lapointe , A.Sarbajna , V. H.Gessner , Acc. Chem. Res. 2022 , 55 , 770–782

2. Reaction monitoring using online vs tube NMR spectroscopy: seriously different results

3. On-line NMR in process engineering

4. Practical aspects of real-time reaction monitoring using multi-nuclear high resolution FlowNMR spectroscopy

5. Online reaction monitoring by single-scan 2D NMR under flow conditions

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