(1S,3S,8R,9S,10R)-9,10-Epoxy-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodecane
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Published:2014-03-26
Issue:4
Volume:70
Page:o480-o480
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ISSN:1600-5368
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Container-title:Acta Crystallographica Section E Structure Reports Online
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language:
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Short-container-title:Acta Cryst E
Author:
Bimoussa Abdoullah,Auhmani Aziz,Ait Itto My Youssef,Daran Jean-Claude,Auhmani Abdelwahed
Abstract
The title compound, C16H26O, was synthesized by treating (1S,3S,8R)-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodec-9-ene with metachloroperbenzoic acid. The molecule is built up from two fused six- and seven-membered rings. The six-membered ring has a half-chair conformation, whereas the seven-membered ring displays a boat conformation. In the crystal, there are no significant intermolecular interactions present.
Publisher
International Union of Crystallography (IUCr)
Subject
Condensed Matter Physics,General Materials Science,General Chemistry
Reference19 articles.
1. Agilent (2012). CrysAlis PRO. Agilent Technologies Ltd, Abingdon, England. 2. SIR97: a new tool for crystal structure determination and refinement 3. (1S,3S,8R,9S)-3,7,7,10-Tétraméthyl-9-[(1S,3S,8R,9S)-3,7,7-triméthyl-10-méthylènetricyclo[6,4,0,01,3]dodéc-9-yloxy]tricyclo[6,4,0,01,3]dodéc-10-ène 4. (1S,3R,8S,9R,10S)-2,2-Dichloro-3,7,7,10-tetramethyl-9,10-epoxytricyclo[6.4.0.01,3]dodecane 5. Identification of the conformational type of seven-membered rings
Cited by
2 articles.
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1. Crystal structure of (1R,3S,8R,11R)-11-acetyl-3,7,7-trimethyl-10-oxatricyclo[6.4.0.01,3]dodecan-9-one;Acta Crystallographica Section E Crystallographic Communications;2015-12-01 2. Crystal structure of (1R,2S,4R,7R,8S,9R)-3,3-dichloro-8,9-epoxy-4,8,12,12-tetramethyltricyclo[5.5.0.02,4]dodecane;Acta Crystallographica Section E Crystallographic Communications;2015-07-04
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