Conversion of Racemic Alkyl Aryl Sulfoxides into Pure Enantiomers Using a Recycle Photoreactor: Tandem Use of Chromatography on Chiral Support and Photoracemization on Solid Support-Reference-Cited by-同舟云学术

Conversion of Racemic Alkyl Aryl Sulfoxides into Pure Enantiomers Using a Recycle Photoreactor: Tandem Use of Chromatography on Chiral Support and Photoracemization on Solid Support

Published:2023-05-08 Issue:11 Volume:88 Page:6955-6961
ISSN:0022-3263
Container-title:The Journal of Organic Chemistry
language:en
Short-container-title:J. Org. Chem.

Author:

Tozawa Kumi¹,Makino Kosho²,Tanaka Yuki¹,Nakamura Kayo¹,Inagaki Akiko³,Tabata Hidetsugu⁴^ORCID,Oshitari Tetsuta⁴^ORCID,Natsugari Hideaki⁵^ORCID,Kuroda Noritaka⁶,Kanemaru Kunio⁷,Oda Yuji⁷,Takahashi Hideyo¹^ORCID

Affiliation:

1. Faculty of Pharmaceutical Sciences, Tokyo University of Science, 2641 Yamazaki, Noda-shi, Chiba 278-8510, Japan

2. Research Institute of Pharmaceutical Sciences, Musashino University, Nishitokyo, Tokyo 202-8585, Japan

3. Faculty of Science and Technology, Seikei University, 3-3-1 Kichijoji Kitamachi, Musashino-shi, Tokyo 180-8633, Japan

4. Faculty of Pharma Sciences, Teikyo University, 2-11-1 Kaga, Itabashi-ku, Tokyo 173-8605, Japan

5. Graduate School of Pharmaceutical Science, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033, Japan

6. YMC Co., Ltd., 284 Daigo, Karasuma Nishiiru Gojo-dori, Shimogyo-ku, Kyoto 600-8106, Japan

7. IWASAKI ELECTRIC CO., LTD., 1-1, Ichiriyama-cho, Gyoda-shi, Saitama 361-8505, Japan

Funder

Japan Science and Technology Agency

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/acs.joc.3c00265

Reference54 articles.

1. Recycle HPLC: A Powerful Tool for the Purification of Natural Products

2. Enantiomeric separation of asymmetric triacylglycerol by recycle high-performance liquid chromatography with chiral column

3. Resolution of a racemic pharmaceutical intermediate

4. Optimal operating policies for closed-loop recycling HPLC processes

5. Preparative chromatographic resolution of racemates on chiral stationary phases on laboratory and production scales by closed-loop recycling chromatography