One‐Pot Catalyst‐Free Direct Sulfenylation of 1‐Aryl Pyrazolones with Aryl Thiols at Room Temperature-Reference-Cited by-同舟云学术

One‐Pot Catalyst‐Free Direct Sulfenylation of 1‐Aryl Pyrazolones with Aryl Thiols at Room Temperature

Published:2017-10-23 Issue:30 Volume:2 Page:9670-9673
ISSN:2365-6549
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language:en
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Author:

Kamani Ronak D.¹,Purohit Vishal B.²,Thummar Rahul P.¹,Sapariya Nirav H.³,Vaghasiya Beena K.¹,Patel Kirit H.¹,Pashavan Chandankumar T.⁴,Shah Manish K.⁴,Raval Dipak K.¹

Affiliation:

1. Department of Chemistry Sardar Patel University Vallabh Vidyanagar- 388120, Gujarat India

2. Shree A. N. Patel P. G. Institute of Science and Research Anand- 388001, Gujarat India

3. Natubhai V. Patel College of Pure and Applied Sciences Vallabh Vidyanagar- 388120, Gujarat India

4. Department of Chemistry Saurashtra University Rajkot- 360005, Gujarat India

Abstract

AbstractA novel strategy for N‐chlorosuccinimide mediated direct sulfenylation of 1‐aryl pyrazolones using aryl thiols has been developed at room temperature. The protocol was found to be simple, efficient and transition metal‐free to afford the target products in good to excellent yields without further purification. The prepared compounds were characterised by 1H NMR, 13C NMR and IR spectroscopy. The skeleton of one of the synthesized compounds has been well confirmed by X‐ray single crystal diffraction (XRD) analysis as well as ORTEP diagram.

Funder

Sardar Patel University

Saurashtra University

Publisher

Wiley

Link

http://onlinelibrary.wiley.com/wol1/doi/10.1002/slct.201701924/fullpdf

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