Gaschromatographic monitoring of volatile pollutants of urban air: optimizing analysis and concentrating

Author:

Denisov I. S.1,Korotkov V. V.1,Smirnov D. S.2

Affiliation:

1. Institution Center of Hygiene and Epidemiology in the Lipetsk region

2. Lipetsk State Technical University

Abstract

For determining 22 volatile organic compounds in the atmospheric air, the operating modes of the gas chromatographic complexes «chromatography-mass spectrometer — two-stage thermodesorber» and «gas chromatograph with 2 FID — static headspace analysis sampler» are optimized. The modes provide the values of the separation coefficients of the chromatographic peaks in the range of 1.5 ÷ 21. It has been experimentally established that the highest desorption efficiency of volatile organic compounds is registered when the sample is concentrated into Tenax TA sorption tubes.

Publisher

PANORAMA Publishing House

Reference7 articles.

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