Synthesis and crystal structure of 3-methyl-2-(methylthio)-4<i>H</i>-chromen-4-one, C<sub>12</sub>H<sub>12</sub>O<sub>2</sub>S-Reference-Cited by-同舟云学术

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Synthesis and crystal structure of 3-methyl-2-(methylthio)-4H-chromen-4-one, C₁₂H₁₂O₂S

Published:2023-05-24 Issue:4 Volume:238 Page:749-750
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Liu Feng¹,Zhang Yuming²,Zhao Zhimeng³,Liu Yi¹,Chen Yang¹,Xiao Tao¹^ORCID

Affiliation:

1. Department of Chemistry and Molecular Engineering , Nanjing Tech University , 30 South Puzhu Road , Nanjing , 211816 , China

2. Changshu Institute of Technology , No. 99 South Third Ring Road (Donghu Campus) , Changshu , 215500 , China

3. School of Environmental Science, Nanjing Xiaozhuang University , 3601 Hongjing Avenue, Jiangning District , Nanjing , 211171 , China

Abstract

Abstract C12H12O2S, monoclinic, P21/c (no. 14), a = 7.4771(1) Å, b = 8.6860(1) Å, c = 16.0445(2) Å, β = 95.374 ( 1 ) ∘

$95.374{\left(1\right)}^{\circ }$

, V = 1037.45(2) Å3, Z = 4, R gt (F) = 0.0311, wR ref (F 2) = 0.1156, T = 293(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0185/pdf

Reference11 articles.

1. Bruker. Apex2, Saint and Sadabs; Bruker AXS Inc.: Madison, Wisconsin, USA, 2012.

2. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystall. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

3. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystall. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

4. Khan, K. M., Ambreen, N., Mughal, U. R., Jalil, S., Perveen, S., Choudhary, M. I. 3-Formylchromones: potential antiinflammatory agents. Eur. J. Med. Chem. 2010, 45, 4058–4064; https://doi.org/10.1016/j.ejmech.2010.05.065.

5. Teimouri, M. B. Serendipitous stereoselective synthesis of brand-new fluorescent dyes: (1Z)-3-(alkylimino)-1-[(chromone-3-yl)methylene]-1,3-dihydro-9H-furo[3,4-b]-chromen-9-one-type fluorophores with blue fluorescence emission properties. Tetrahedron 2011, 67, 1837–1843; https://doi.org/10.1016/j.tet.2011.01.033.

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